2D CC-CTUC Solids

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	}}		}}
	===CO-CA Version===		===CO-CA Version===
-	<pulse test=true>	+	<pulse>
	anchors: @a,a1,a2 @b,b1 @c @c1,d,d1 @e @f @g @h------h1 @i		anchors: @a,a1,a2 @b,b1 @c @c1,d,d1 @e @f @g @h------h1 @i
	disp: 4@a 5@b 7@c 7@d 1@e 7@f 7@g 4@h 10@i		disp: 4@a 5@b 7@c 7@d 1@e 7@f 7@g 4@h 10@i
	time: rlx @a t1 @b t2 @c t3 @d t4 @e t5 @f t5 @g t6 @h d @i		time: rlx @a t1 @b t2 @c t3 @d t4 @e t5 @f t5 @g t6 @h d @i
-	rf H: 90@a wp@a1,b=irr wp@b1------------------------------------------g wp@h1----i	+	rf H: 90@a wp@a1,b=irr wp@b1--------------------------------------g wp@h1----i
	rf 13C: wp@a2,b 180@c 90@d 90@e 180@f 90@g 90@h acq@h1----i		rf 13C: wp@a2,b 180@c 90@d 90@e 180@f 90@g 90@h acq@h1----i
	rf 15N: wp@h1----i		rf 15N: wp@h1----i

---

Revision as of 01:28, 4 September 2008

Name: hCC-2D-DARR
Experiment family/families: solids
Synopsis: Simple Carbon or Nitrogen 2D experiment with DARR (RAD) broadband mixing
Implementation author(s): L. Chen, D.W. Elliot, J.M. Boetcher, D.H. Zhou, C.M. Rienstra, L.J. Mueller
Copyright: not assigned
Console: Varian, Infinity Plus, 500 MHz
Download: code, no sample/parameter data yet

CO-CA Version

Aliphatic Version

References

1. Lee, YK and Kurur, ND and Helmle, M and Johannessen, OG and Nielsen, NC and Levitt, MH. Efficient dipolar recoupling in the NMR of rotating solids. A sevenfold symmetric radiofrequency pulse sequence. Chemical Physics Letters 242(3):304--309, 1995. BibTeX [levitt95]

2. Hohwy, M and Jakobsen, HJ and Ed{\'e}n, M and Levitt, MH and Nielsen, NC. Broadband dipolar recoupling in the nuclear magnetic resonance of rotating solids: A compensated C7 pulse sequence. The Journal of Chemical Physics 108:2686, 1998. BibTeX [postc7]

3. Rienstra, CM and Hatcher, ME and Mueller, LJ and Sun, B and Fesik, SW and Griffin, RG. Efficient Multispin Homonuclear Double-Quantum Recoupling for Magic-Angle Spinning NMR:\^{} 1\^{} 3C-\^{} 1\^{} 3C Correlation Spectroscopy of U-\^{} 1\^{} 3C-Erythromycin A. Journal of the American Chemical Society 120:10602--10612, 1998. BibTeX [cmr7]

4. Hohwy, M and Rienstra, CM and Jaroniec, CP and Griffin, RG. Fivefold symmetric homonuclear dipolar recoupling in rotating solids: Application to double quantum spectroscopy. The Journal of Chemical Physics 110:7983, 1999. BibTeX [spc5]