2D CC-CTUC Solids

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|observe=C
|observe=C
}}
}}
 +
# CO-CA Version
<pulse>
<pulse>
anchors: @a,a1,a2 @b,b1 @c @c1,d,d1 @e @f @g @h,h1,h2,h3 @i
anchors: @a,a1,a2 @b,b1 @c @c1,d,d1 @e @f @g @h,h1,h2,h3 @i
Line 19: Line 20:
time: rlx @a t1 @b t2 @c t3 @d t4 @e t5 @f t5 @g t6 @h d @i
time: rlx @a t1 @b t2 @c t3 @d t4 @e t5 @f t5 @g t6 @h d @i
-
rf H: 90@a wp@a1,b wp@b1--h wp@h1--i
+
rf H: 90@a wp@a1,b wp@b1--g wp@h1--i
rf 13C: wp@a2,b 180@c 90@d 90@e 180@f 90@g 90@h acq@h2---------i
rf 13C: wp@a2,b 180@c 90@d 90@e 180@f 90@g 90@h acq@h2---------i
rf 15N: wp@h3,i
rf 15N: wp@h3,i
Line 43: Line 44:
phase phi2: label=\phi_2 table=1,3
phase phi2: label=\phi_2 table=1,3
</pulse>
</pulse>
-
 
+
# Aliphatic Version
<pulse>
<pulse>
-
anchors: @a,a1,a2 @b,b1 @c @c1,d,d1 @e @f @g @h,h1,h2,h3 @i,i2 @j
+
anchors: @a,a1,a2 @b,b1 @c @c1,d,d1 @e @f @g @h,h1,h2,h3 @i,i1,i2,i3 @j
-
disp: 4@a 5@b 10@c 5@d 10@e 1@f 10@g 10@h 4@i 10@j
+
disp: 4@a 5@b 7@c 7@d 7@e 1@f 5@g 5@h 4@i 10@j
-
time: rlx @a t1 @b t2 @c t3 @d t4 @e t5 @f t5 @g t6 @h d @i d @j
+
time: rlx @a t1 @b t2 @c t3 @d t4 @e t5 @f t4 @g t4 @h t6 @i d @j
-
rf H: 90@a wp@a1,b wp@b1--h wp@h1--j
+
rf H: 90@a wp@a1,b wp@b1--h wp@i1--j
rf 13Cali: wp@a2,b shp@c 90@e 90@f shp@g 90@h 90@i acq@i2---------j
rf 13Cali: wp@a2,b shp@c 90@e 90@f shp@g 90@h 90@i acq@i2---------j
rf 13CO: wp@a2,b shp@d 90@e 90@f 90@h 90@i
rf 13CO: wp@a2,b shp@d 90@e 90@f 90@h 90@i
-
rf 15N: wp@h3,j
+
rf 15N: wp@i3,j
delay t1: show_at=13Cali label=ct
delay t1: show_at=13Cali label=ct
delay t2: show_at=13Cali label=\tau-\frac{t_1}{2}
delay t2: show_at=13Cali label=\tau-\frac{t_1}{2}
delay t3: show_at=13Cali label=\tau+\frac{t_1}{2}
delay t3: show_at=13Cali label=\tau+\frac{t_1}{2}
-
delay t4: hide=true
+
delay t4: show_at=13Cali label=\tau
-
delay t5: show_at=13Cali label=\tau
+
delay t5: hide=true
delay t6: show_at=13Cali label=\tau_{zf}
delay t6: show_at=13Cali label=\tau_{zf}

Revision as of 22:13, 3 September 2008

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Name: hCC-2D-DARR
Experiment family/families: solids
Synopsis: Simple Carbon or Nitrogen 2D experiment with DARR (RAD) broadband mixing
Implementation author(s): L. Chen, D.W. Elliot, J.M. Boetcher, D.H. Zhou, C.M. Rienstra, L.J. Mueller
Copyright: not assigned
Console: Varian, Infinity Plus, 500 MHz
Download: code, no sample/parameter data yet
  1. CO-CA Version

Pulse sequence image

  1. Aliphatic Version

Pulse sequence image

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