2D CC-CTUC Solids
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(Difference between revisions)
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|observe=C | |observe=C | ||
}} | }} | ||
+ | # CO-CA Version | ||
<pulse> | <pulse> | ||
anchors: @a,a1,a2 @b,b1 @c @c1,d,d1 @e @f @g @h,h1,h2,h3 @i | anchors: @a,a1,a2 @b,b1 @c @c1,d,d1 @e @f @g @h,h1,h2,h3 @i | ||
Line 19: | Line 20: | ||
time: rlx @a t1 @b t2 @c t3 @d t4 @e t5 @f t5 @g t6 @h d @i | time: rlx @a t1 @b t2 @c t3 @d t4 @e t5 @f t5 @g t6 @h d @i | ||
- | rf H: 90@a wp@a1,b wp@b1-- | + | rf H: 90@a wp@a1,b wp@b1--g wp@h1--i |
rf 13C: wp@a2,b 180@c 90@d 90@e 180@f 90@g 90@h acq@h2---------i | rf 13C: wp@a2,b 180@c 90@d 90@e 180@f 90@g 90@h acq@h2---------i | ||
rf 15N: wp@h3,i | rf 15N: wp@h3,i | ||
Line 43: | Line 44: | ||
phase phi2: label=\phi_2 table=1,3 | phase phi2: label=\phi_2 table=1,3 | ||
</pulse> | </pulse> | ||
- | + | # Aliphatic Version | |
<pulse> | <pulse> | ||
- | anchors: @a,a1,a2 @b,b1 @c @c1,d,d1 @e @f @g @h,h1,h2,h3 @i,i2 @j | + | anchors: @a,a1,a2 @b,b1 @c @c1,d,d1 @e @f @g @h,h1,h2,h3 @i,i1,i2,i3 @j |
- | disp: 4@a 5@b | + | disp: 4@a 5@b 7@c 7@d 7@e 1@f 5@g 5@h 4@i 10@j |
- | time: rlx @a t1 @b t2 @c t3 @d t4 @e t5 @f | + | time: rlx @a t1 @b t2 @c t3 @d t4 @e t5 @f t4 @g t4 @h t6 @i d @j |
- | rf H: 90@a wp@a1,b wp@b1--h wp@ | + | rf H: 90@a wp@a1,b wp@b1--h wp@i1--j |
rf 13Cali: wp@a2,b shp@c 90@e 90@f shp@g 90@h 90@i acq@i2---------j | rf 13Cali: wp@a2,b shp@c 90@e 90@f shp@g 90@h 90@i acq@i2---------j | ||
rf 13CO: wp@a2,b shp@d 90@e 90@f 90@h 90@i | rf 13CO: wp@a2,b shp@d 90@e 90@f 90@h 90@i | ||
- | rf 15N: wp@ | + | rf 15N: wp@i3,j |
delay t1: show_at=13Cali label=ct | delay t1: show_at=13Cali label=ct | ||
delay t2: show_at=13Cali label=\tau-\frac{t_1}{2} | delay t2: show_at=13Cali label=\tau-\frac{t_1}{2} | ||
delay t3: show_at=13Cali label=\tau+\frac{t_1}{2} | delay t3: show_at=13Cali label=\tau+\frac{t_1}{2} | ||
- | delay t4 | + | delay t4: show_at=13Cali label=\tau |
- | + | delay t5: hide=true | |
delay t6: show_at=13Cali label=\tau_{zf} | delay t6: show_at=13Cali label=\tau_{zf} | ||
Revision as of 22:13, 3 September 2008
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Experiment family/families: solids
Synopsis: Simple Carbon or Nitrogen 2D experiment with DARR (RAD) broadband mixing
Implementation author(s): L. Chen, D.W. Elliot, J.M. Boetcher, D.H. Zhou, C.M. Rienstra, L.J. Mueller
Copyright: not assigned
Console: Varian, Infinity Plus, 500 MHz
Download: code, no sample/parameter data yet
- CO-CA Version
- Aliphatic Version
Categories: Pulse sequences | UIUC pulse sequences | Varian | Solids | Infinity Plus | 500 MHz | 1H | 15N | 13C | Heteronuclear | 13C detected | 2D