# 2D CC-CTUC Solids

(Difference between revisions)
 Revision as of 21:00, 4 September 2008 (edit)← Previous diff Revision as of 21:45, 4 September 2008 (edit) (undo)Next diff → Line 20: Line 20: time: rlx @a t1 @b t2 @c t3 @d t4 @e t5 @f t5 @g t6 @h d @i time: rlx @a t1 @b t2 @c t3 @d t4 @e t5 @f t5 @g t6 @h d @i - rf H: 90@a wp@a1,b=irr wp@b1--------------------------------------g=fulldec wp@h1----i=acqdec + rf H: 90@a=phy wp@a1,b=posramp wp@b1--------------------------------------g=fulldec wp@h1----i=acqdec - rf 13C: wp@a2,b=posramp 180@c 90@d 90@e 180@f 90@g 90@h acq@h1----i + rf 13C: wp@a2,b=irr 180@c=phx 90@d=phy 90@e=phx 180@f=phy 90@g=phx 90@h=phmx acq@h1----i rf 15N: wp@h1----i rf 15N: wp@h1----i Line 30: Line 30: delay t5: show_at=13C label=\tau delay t5: show_at=13C label=\tau delay t6: show_at=13C label=\tau_{zf} delay t6: show_at=13C label=\tau_{zf} + + pulse p1: phase=phi1 + + pulse phx: phase=px + pulse phmx: phase=mx + pulse phy: phase=py + + phase px: label=x + phase py: label=y + phase mx: label=-x delay rlx: hide=true delay rlx: hide=true Line 39: Line 49: pulse p1: phase=phi1 pulse p1: phase=phi1 - wp irr: h1=65 + wp irr: h1=65 label=x - wp posramp: h1=65 h2=95 + wp posramp: h1=65 h2=95 label=x wp fulldec: h1=100 label=SPINAL wp fulldec: h1=100 label=SPINAL wp acqdec: h1=75 label=SPINAL wp acqdec: h1=75 label=SPINAL Line 85: Line 95: phase phi2: label=\phi_2 table=1,3 phase phi2: label=\phi_2 table=1,3 + + ===CACO IPAP (IP) Version=== + + anchors: @a,a1,a2 @b,b1 @c @c1,d,d1 @e @f @g @h------h1 @i + disp: 4@a 5@b 7@c 7@d 1@e 7@f 7@g 4@h 10@i + time: rlx @a t1 @b t2 @c t3 @d t4 @e t5 @f t5 @g t6 @h d @i + + rf H: 90@a wp@a1,b=irr wp@b1--------------------------------------g=fulldec wp@h1----i=acqdec + rf 13C: wp@a2,b=posramp 180@c 90@d 90@e 180@f 90@g 90@h acq@h1----i + rf 15N: wp@h1----i + + delay t1: show_at=13C label=ct label_yoffset=-30 + delay t2: show_at=13C label=\tau_1-\frac{t_1}{2} + delay t3: show_at=13C label=\tau_1+\frac{t_1}{2} + delay t4: hide=true + delay t5: show_at=13C label=\tau_2 + delay t6: show_at=13C label=\tau_{zf} + + delay rlx: hide=true + delay d: hide=true + + rfchan 13C: label=^{13}C + rfchan 15N: label=^{15}N + rfchan H: label=^1H + + pulse p1: phase=phi1 + wp irr: h1=65 + wp posramp: h1=65 h2=95 + wp fulldec: h1=100 label=SPINAL + wp acqdec: h1=75 label=SPINAL + acq: phase=phi2 type=fid + + phase phi1: table=0,2 label=\phi_1 + phase phi2: label=\phi_2 table=1,3 + + + ===CACO IPAP (AP) Version=== + + anchors: @a,a1,a2 @b,b1 @c @c1,d,d1 @e @f @g @h------h1 @i + disp: 4@a 5@b 7@c 7@d 1@e 7@f 7@g 4@h 10@i + time: rlx @a t1 @b t2 @c t3 @d t4 @e t5 @f t5 @g t6 @h d @i + + rf H: 90@a wp@a1,b=irr wp@b1--------------------------------------g=fulldec wp@h1----i=acqdec + rf 13C: wp@a2,b=posramp 180@c 90@d 90@e shp@f=COsoft acq@h1----i + rf 15N: wp@h1----i + + delay t1: show_at=13C label=ct label_yoffset=-30 + delay t2: show_at=13C label=\tau_1-\frac{t_1}{2} + delay t3: show_at=13C label=\tau_1+\frac{t_1}{2} + delay t4: hide=true + delay t5: show_at=13C label=\tau_2 + delay t6: show_at=13C label=\tau_{zf} + + delay rlx: hide=true + delay d: hide=true + + rfchan 13C: label=^{13}C + rfchan 15N: label=^{15}N + rfchan H: label=^1H + + pulse p1: phase=phi1 + wp irr: h1=65 + wp posramp: h1=65 h2=95 + wp fulldec: h1=100 label=SPINAL + wp acqdec: h1=75 label=SPINAL + acq: phase=phi2 type=fid + + phase phi1: table=0,2 label=\phi_1 + phase phi2: label=\phi_2 table=1,3 + + ==References== ==References==

## Revision as of 21:45, 4 September 2008

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Name: hCC-2D-CTUC COSY
Experiment family/families: solids
Synopsis: Constant-time Through-bond Carbon 2D correlation experiments
Implementation author(s): L. Chen, D.W. Elliot, J.M. Boetcher, D.H. Zhou, C.M. Rienstra, L.J. Mueller
Console: Varian, Infinity Plus, 500 MHz