2D CC-CTUC Solids

From NMR Wiki

(Difference between revisions)
Jump to: navigation, search
Line 22: Line 22:
The next several files should be separated and placed in /export/homes/USERNAME/pulse_sequences/cpc/includes. Each new file begins with a long comment section.
The next several files should be separated and placed in /export/homes/USERNAME/pulse_sequences/cpc/includes. Each new file begins with a long comment section.
-
The files acq.inc, CTUC_COSY.acq, CTUC_COSY.s, rSNOB_063108.inc, rSNOB_delay2.incSPC5.inc, SPINAL1.inc, SPINAL2.inc, STANDARD_PARAMS, std_errs.inc, t1.inc, t2.inc, TAN_CP.inc, and TWO_D.inc should be created from this file.
+
The files acq.inc, CTUC_COSY.acq, CTUC_COSY.s, rSNOB_063108.inc, rSNOB_delay2.incSPC5.inc, [http://nmrwiki.org/wiki/images/6/69/SPINAL1.inc.txt SPINAL1.inc], SPINAL2.inc, STANDARD_PARAMS, std_errs.inc, t1.inc, t2.inc, TAN_CP.inc, and TWO_D.inc should be created from this file.
===CO-CA Version===
===CO-CA Version===

Revision as of 16:45, 5 September 2008

This page is a part of the user-editable NMR Wiki pulse sequence database.

Disclaimer: You are solely responsible for correct use of these materials on your instrument.

Ps.DB

search database
help.edit.pulsesequence.record

see edit instructions
help.adding.pulse.sequence

see deposition instructions
report.suggestions

report suggestions
Name: hCC-2D-CTUC COSY
Experiment family/families: solids
Synopsis: Constant-time Through-bond Carbon 2D correlation experiments
Implementation author(s): Lindsay Sperling, Gemma Commellas, Trent Franks, Chad Rienstra
Copyright: not assigned
Console: Varian, Infinity Plus, 500 MHz
Download: code, no sample/parameter data yet

Implementation

All needed files were catenated together, and so must be separated. The file CTUC_COSY.acq is the first block of text after the author contributions. CTUC_COSY.s begins with

    name	"2D_CC_shell";

and ends with

    return;

The next several files should be separated and placed in /export/homes/USERNAME/pulse_sequences/cpc/includes. Each new file begins with a long comment section. The files acq.inc, CTUC_COSY.acq, CTUC_COSY.s, rSNOB_063108.inc, rSNOB_delay2.incSPC5.inc, SPINAL1.inc, SPINAL2.inc, STANDARD_PARAMS, std_errs.inc, t1.inc, t2.inc, TAN_CP.inc, and TWO_D.inc should be created from this file.

CO-CA Version

The hard pulse version of the experiment can be used if soft_pulse_flag=0 and ipap_flag=0.

Pulse sequence image

Aliphatic Version

The soft pulse version of the experiment can be used if soft_pulse_flag=1 and ipap_flag=0.

Pulse sequence image

CACO IPAP (IP) Version

The IP version of the experiment can be used if soft_pulse_flag=0 and ipap_flag=0, with the carrier placed on resonance with the Carbonyl frequency.

Pulse sequence image

CACO IPAP (AP) Version

The AP version of the experiment can be used if ipap_flag=1 (independent of soft_pulse_flag), with the carrier placed on resonance with the Carbonyl frequency.

Pulse sequence image


References

  1. Chen, L and Olson, RA and Elliot, DW and Boettcher, JM and Zhou, DH and Rienstra, CM and Mueller, LJ. Constant-Time Through-Bond ^{13}C Correlation Spectroscopy for Assigning Protein Resonances with Solid-State NMR Spectroscopy. J Am Chem Soc 128(31):9992--9993, 2006. BibTeX [bbCTUC]
  2. Chen, L and Kaiser, JM and Lai, J and Polenova, T and Yang, J and Rienstra, CM and Mueller, LJ. J-based 2D homonuclear and heteronuclear correlation in solid-state proteins. Magn Reson Chem 45 suppl.:s84-s92, 2007. BibTeX [ipapCTUC]

Personal tools