Oneshot for Bruker (G.A. Morris/M. Nilsson)
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Basic facts about Oneshot
Synopsis: 2D Oneshot DOSY pulse sequence
Family: Diffusion experiments
Copyright: Manchester University
Sample data (available through "parameters" link above) was recorded at 300K
- D-(-)-Fructose: 182 mM
- Propan-1-ol: 316 mM
- D2O: 0.8 mL
- TSP for δ scale reference
Experiments (included in the parameters archive):
- 10 - 1D 1H.
- 11 - Doneshot 16 transients. 18 minutes.
- 15 - Doneshot 1 transient. 38 seconds.
DOSY data above was processed with DOSY toolbox for Matlab.
Setup of the pulse sequence in Topspin is described in this pdf document.