Dry air/gases for analytical instruments

From NMR Wiki

Revision as of 23:08, 2 December 2008 by Evgeny Fadeev (Talk | contribs)
Jump to: navigation, search

Stream of dry gases (air or nitrogen) are used in the practice of NMR spectroscopy to regulate sample temperature.

Typically gas is cooled to some temperature that is lower then the desired sample temperature. Cooled gas is then passed through electric heater where it reaches the target temperature and then comes in contact with the sample.

Dew point of gas is an important parameter to consider. Dew point should be 20oC below the lowest temperature anywhere in the path of the gas stream [1].

Contents

Dew point sensing

modelrangeprecisionnotes
GE DewPro MMY30 -130oF to 500F (-90 to 10oC) 2oC
  • has digital display
  • requires recalibration every 6 months for max accuracy, once a year for 5oC accuracy
  • cost ~$2,700

Dessicant dryers

Pressure Swing Adsorption dryers

Membrane dryers

Refrigeration dryers

Manufacturers

Hankison, Inc.

References

  1. Instruction manual for FTS XR401 Air-Jet crystal cooler [xr401]
Personal tools