SPINAL
From NMR Wiki
SPINAL Decoupling
SPINAL decoupling is an extension of TPPM. SPINAL can be thought of as TPPM with a supercycle. Like TPPM, the pulse width must be optimized once a decoupling amplitude has been set. The phases are generally set to 5, 10, and 15, however in this implementation the user has the option to change each phase as they see fit. The SPINAL supercycle is chosen through the spinal_flag variable. when the flag is zero, it is TPPM decoupling, 1=SPINAL8, 2=SPINAL16, 3=SPINAL32 and 4=SPINAL64. When alpha=beta=0 and phi(SPINAL) = 1/2 phi(TPPM) the result is also very near to TPPM decoupling.
This page is a part of the user-editable NMR Wiki pulse sequence database.
Disclaimer: You are solely responsible for correct use of these materials on your instrument.
search database | see edit instructions | see deposition instructions | report suggestions |
Experiment family/families: solids
Synopsis: Includes file for SPINAL decoupling
Implementation author(s): Benjamin Wylie, Trent Franks, Chad Rienstra
Copyright: not assigned
Console: Varian, Infinity Plus, 500 MHz
Download: code, no sample/parameter data yet
This page is a part of the user-editable NMR Wiki pulse sequence database.
Disclaimer: You are solely responsible for correct use of these materials on your instrument.
search database | see edit instructions | see deposition instructions | report suggestions |
Experiment family/families: solids
Synopsis: Includes file for SPINAL decoupling
Implementation author(s): Benjamin Wylie, Trent Franks, Chad Rienstra
Copyright: not assigned
Console: Varian, Infinity Plus, 500 MHz
Download: code, no sample/parameter data yet
References
- Fung, BM and Khitrin, AK and Ermolaev, K. An Improved Broadband Decoupling Sequence for Liquid Crystals and Solids. J Magn Reson 142(31):97-101, 2000. BibTeX
Categories: Pulse sequences | UIUC pulse sequences | Varian | Solids | Infinity Plus | 500 MHz | 1H | 1H detected | Homonuclear | MAS | ChemMagnetics