2D CC-CTUC Solids
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(Difference between revisions)
Line 34: | Line 34: | ||
rfchan 13C: label=^{13}C | rfchan 13C: label=^{13}C | ||
+ | rfchan 15N: label=^{15}N | ||
+ | rfchan H: label=^1H | ||
+ | |||
+ | pulse p1: phase=phi1 | ||
+ | acq: phase=phi2 type=fid | ||
+ | |||
+ | phase phi1: table=0,2 label=\phi_1 | ||
+ | phase phi2: label=\phi_2 table=1,3 | ||
+ | </pulse> | ||
+ | |||
+ | <pulse> | ||
+ | anchors: @a,a1,a2 @b,b1 @c @c1,d,d1 @e @f @g @h,h1,h2,h3 @i,i2 @j | ||
+ | disp: 4@a 5@b 10@c 5@d 10@e 1@f 10@g 10@h 4@i 10@j | ||
+ | time: rlx @a t1 @b t2 @c t3 @d t4 @e t5 @f t5 @g t6 @h d @i d @j | ||
+ | |||
+ | rf H: 90@a wp@a1,b wp@b1--h wp@h1--j | ||
+ | rf 13Cali: wp@a2,b shp@c 90@e 90@f shp@g 90@h 90@i acq@i2---------j | ||
+ | rf 13CO: wp@a2,b shp@d 90@e 90@f 90@h 90@i | ||
+ | rf 15N: wp@h3,j | ||
+ | |||
+ | delay t1: show_at=13Cali label=ct | ||
+ | delay t2: show_at=13Cali label=\tau-\frac{t_1}{2} | ||
+ | delay t3: show_at=13Cali label=\tau+\frac{t_1}{2} | ||
+ | delay t4: hide=true | ||
+ | delay t5: show_at=13Cali label=\tau | ||
+ | delay t6: show_at=13Cali label=\tau_{zf} | ||
+ | |||
+ | delay rlx: hide=true | ||
+ | delay d: hide=true | ||
+ | |||
+ | rfchan 13Cali: label=^{13}C_{Aliphatic} | ||
+ | rfchan 13CO: label=^{13}C_{Carbonyl} | ||
rfchan 15N: label=^{15}N | rfchan 15N: label=^{15}N | ||
rfchan H: label=^1H | rfchan H: label=^1H |
Revision as of 21:41, 3 September 2008
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Experiment family/families: solids
Synopsis: Simple Carbon or Nitrogen 2D experiment with DARR (RAD) broadband mixing
Implementation author(s): L. Chen, D.W. Elliot, J.M. Boetcher, D.H. Zhou, C.M. Rienstra, L.J. Mueller
Copyright: not assigned
Console: Varian, Infinity Plus, 500 MHz
Download: code, no sample/parameter data yet
Categories: Pulse sequences | UIUC pulse sequences | Varian | Solids | Infinity Plus | 500 MHz | 1H | 15N | 13C | Heteronuclear | 13C detected | 2D