Oneshot for Bruker (G.A. Morris/M. Nilsson)
From NMR Wiki
This page is a part of the user-editable NMR Wiki pulse sequence database.
Disclaimer: You are solely responsible for correct use of these materials on your instrument.
search database | see edit instructions | see deposition instructions | report suggestions |
Basic facts about Oneshot
Synopsis: 2D Oneshot DOSY pulse sequence | ||||
Family: Diffusion experiments | ||||
| ||||
Copyright: Manchester University |
Sample data
Sample data (available through "parameters" link above) was recorded at 300K
Sample composition:
- D-(-)-Fructose: 182 mM
- Propan-1-ol: 316 mM
- D2O: 0.8 mL
- TSP for δ scale reference
Experiments (included in the parameters archive):
- 10 - 1D 1H.
- 11 - Doneshot 16 transients. 18 minutes.
- 15 - Doneshot 1 transient. 38 seconds.
DOSY spectrum. |
DOSY spectrum. |
DOSY data above was processed with DOSY toolbox for Matlab.
Setup instructions
Setup of the pulse sequence in Topspin is described in this pdf document.
Categories: Pulse sequences | Liquids | Bruker | GA Morris/M Nilsson Labs | 1H detected | 2D | DOSY | Diffusion | Oneshot | PFG